Sample preparation procedure for the

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Jun 7, 2011 - of polycyclic aromatic hydrocarbons in petroleum vacuum ...... lubricating base oils and asphaltene free petroleum fractions— dimethyl ...
Anal Bioanal Chem (2011) 401:1059–1069 DOI 10.1007/s00216-011-5134-9

ORIGINAL PAPER

Sample preparation procedure for the determination of polycyclic aromatic hydrocarbons in petroleum vacuum residue and bitumen Ewelina Gilgenast & Grzegorz Boczkaj & Andrzej Przyjazny & Marian Kamiński

Received: 11 April 2011 / Revised: 20 May 2011 / Accepted: 20 May 2011 / Published online: 7 June 2011 # The Author(s) 2011. This article is published with open access at Springerlink.com

Abstract This paper describes a novel method of sample preparation for the determination of trace concentrations of polycyclic aromatic hydrocarbons (PAHs) in high-boiling petroleum products. Limits of quantitation of the investigated PAHs in materials of this type range from tens of nanograms per kilogram to