Jun 7, 2011 - of polycyclic aromatic hydrocarbons in petroleum vacuum ...... lubricating base oils and asphaltene free petroleum fractionsâ dimethyl ...
Anal Bioanal Chem (2011) 401:1059–1069 DOI 10.1007/s00216-011-5134-9
ORIGINAL PAPER
Sample preparation procedure for the determination of polycyclic aromatic hydrocarbons in petroleum vacuum residue and bitumen Ewelina Gilgenast & Grzegorz Boczkaj & Andrzej Przyjazny & Marian Kamiński
Received: 11 April 2011 / Revised: 20 May 2011 / Accepted: 20 May 2011 / Published online: 7 June 2011 # The Author(s) 2011. This article is published with open access at Springerlink.com
Abstract This paper describes a novel method of sample preparation for the determination of trace concentrations of polycyclic aromatic hydrocarbons (PAHs) in high-boiling petroleum products. Limits of quantitation of the investigated PAHs in materials of this type range from tens of nanograms per kilogram to